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标题: 请教一下,USP中水浴加热水浴温度应该为多少? [打印本页]

作者: meimei7071    时间: 2015-3-6 12:06 PM
标题: 请教一下,USP中水浴加热水浴温度应该为多少?
Pipet 10 mL of the substrate solution, stand at 37±0.50 for 10 minutes, add exactly 1 mL of the sample solu-tion, and shake immediately. Allow this solution to stand at37±0.5 C for exactly 10 minutes, add exactly 2 mL of alkaline tartrate solution of the Fehling's TS for amylolytic activity test, and shake immediately. Then, add exactly 2 mL of copper solution of the Fehling's TS for amylolytic activity( A, A9 w* L& I' K# L3 g
test, shake gently, heat the solution in a water bath for ex-actly 15 minutes, and then immediately cool to below 25 C.Then, add exactly 2 mL of concentrated potassium iodide TS and2mLofdilutedsulfuricacid(1in6), andtitrat the released iodine with 0.05 mol/L sodium thiosulfate VS to the disappearance of the blue color produced by addition of 1 to 2 drops of soluble starch TS (amL). Separately, pipet 10 mL of water instead of the substrate solution and titrate <2.50>inthesamemanner(bmL).
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' y+ b) `! o& ^% g+ N; W# M请教一下,文中heat the solution in a water bath for eactly 15 minutes, 水浴加热中水浴的温度应该为多少呢?
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作者: ZGZG    时间: 2015-3-6 03:37 PM
,Ch.p是98-100度
作者: 黑龙    时间: 2015-3-6 04:38 PM
应该是100吧
作者: meimei7071    时间: 2015-3-9 12:05 PM
谢谢各位了




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